N,N′-Di-8-quinolyl-2,2′-(o-phenylenedioxy)diacetamide

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N,N′-Di-8-quinolyl-2,2′-(o-phenyl­ene­di­oxy)diacetamide

In the title compound, C(28)H(22)N(4)O(4), the mol-ecule lies on a crystallographic twofold axis. The quinoline ring is essentially planar (give max or rms deviation 0.0186 Å), and the dihedral angle between the quinoline ring and the central benzene ring is 19.1 (4)°. Intra-molecular N-H⋯(N,O) and C-H⋯O hydrogen bonds contribute to the formation of the roughly planar configuration. The crystal...

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2-Nitro-N-(8-quinolyl)benzamide

In the title compound, C(16)H(11)N(3)O(3), the amide group is twisted away from the quinoline ring system and nitro-benzene ring by 8.02 (1)° and 54.92 (1)°, respectively. The crystal packing is stabilized by inter-molecular C-H⋯O hydrogen bonds, and π-π inter-actions between the quinoline ring systems of inversion-related mol-ecules, with a centroid-centroid distance of 3.4802 (13) Å.

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8-Quinolyl 5-(dimethyl­amino)­naphthalene-1-sulfonate

In the title compound, C(21)H(18)N(2)O(3)S, the dihedral angle between the naphthalene and quinoline ring systems is 55.53 (2)°, and the torsion angle involving the connecting C-S-O-C atoms is 87.60 (3)°. In the crystal structure, weak inter-molecular C-H⋯O hydrogen bonds connect mol-ecules into chains along [100] and there are π-π stacking inter-actions between pairs of chains with a centroid-...

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(E)-2-[2-(Penta­fluoro­phen­yl)ethen­yl]-8-quinolyl acetate

The title compound, C(19)H(10)F(5)NO(2), was synthesized by the 1:1 condensation of 2-methyl-8-hydroxy-quinaldine with penta-fluoro-benzaldehyde. It crystallizes with two almost identical mol-ecules in the asymmetric unit. The penta-fluoro-benzene ring is essentially coplanar with the quinoline ring, forming dihedral angles of 2.49 (17) and 8.72 (16)° in the two mol-ecules.

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(E)-2-[2-(2-Nitro­phen­yl)ethen­yl]-8-quinolyl acetate

The title compound, C(19)H(14)N(2)O(4), crystallizes with two molecules with very similar conformations in the asymmetric unit; the angles between the two ring systems are 8.7 (1) and 4.2 (1)°. In the crystal, inter-molecular π-π inter-actions [centroid-centroid distance 3.973 (1) Å] lead to a three-dimensional network.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2009

ISSN: 1600-5368

DOI: 10.1107/s1600536809041312